Nuclear magnetic resonance crystallography information
Nuclear magnetic resonance crystallography (NMR crystallography) is a method which utilizes primarily NMR spectroscopy to determine the structure of solid materials on the atomic scale. Thus, solid-state NMR spectroscopy would be used primarily, possibly supplemented by quantum chemistry calculations (e.g. density functional theory),[1] powder diffraction[2] etc. If suitable crystals can be grown, any crystallographic method would generally be preferred to determine the crystal structure comprising in case of organic compounds the molecular structures and molecular packing. The main interest in NMR crystallography is in microcrystalline materials which are amenable to this method but not to X-ray, neutron and electron diffraction. This is largely because interactions of comparably short range are measured in NMR crystallography.
^Robinson, Philip (26 February 2009). "Crystal clear method for identifying powders". Highlights in Chemical Technology. Retrieved 2015-10-22.
^Harris KDM, Xu M (2009). Combined Analysis of NMR & Powder Diffraction Data. Wiley-Blackwell. ISBN 978-0-470-69961-4.
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