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Powder diffraction information


Electron powder pattern (red) of an Al film with an fcc spiral overlay (green) and a line of intersections (blue) that determines lattice parameter.[1]
X-ray powder diffraction of Y2Cu2O5 and Rietveld refinement with two phases, showing 1% of yttrium oxide impurity (red tickers).
X-ray powder diffraction of Y2Cu2O5 and Rietveld refinement with two phases, showing 1% of yttrium oxide impurity (red tickers).

Powder diffraction is a scientific technique using X-ray, neutron, or electron diffraction on powder or microcrystalline samples for structural characterization of materials.[2] An instrument dedicated to performing such powder measurements is called a powder diffractometer.

Powder diffraction stands in contrast to single crystal diffraction techniques, which work best with a single, well-ordered crystal.

  1. ^ P. Fraundorf & Shuhan Lin (2004). "Spiral powder overlays". Microscopy and Microanalysis. 10 (S02): 1356–1357. Bibcode:2004MiMic..10S1356F. doi:10.1017/S1431927604884034. S2CID 17009500.
  2. ^ B.D. Cullity Elements of X-ray Diffraction Addison Wesley Mass. 1978 ISBN 0-201-01174-3

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Powder diffraction

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Powder diffraction is a scientific technique using X-ray, neutron, or electron diffraction on powder or microcrystalline samples for structural characterization...

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International Centre for Diffraction Data

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International Centre for Diffraction Data (ICDD) maintains a database of powder diffraction patterns, the Powder Diffraction File (PDF), including the...

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Rietveld refinement

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transfer Q, which is historically rarely used in powder diffraction but very common in all other diffraction and optics techniques. The relation is Q = 4...

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Neutron diffraction

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making neutron diffraction an important tool of crystallography. Neutron diffraction is closely related to X-ray powder diffraction. In fact, the single...

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Mineralogy

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(2008). "1. Principles of powder diffraction". In Dinnebier, Robert E.; Billinge, Simon J.L. (eds.). Powder diffraction : theory and practice (Repr...

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Selected area diffraction

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times larger, the electrons are diffracted on the crystal lattice, acting as a diffraction grating. Due to the diffraction, part of the electrons is scattered...

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Crystallographic database

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reflection intensities and lattice spacings from X-ray powder diffraction data with entries in powder-diffraction fingerprinting databases. Crystal structures of...

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Electron diffraction

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overview of electron diffraction and electron diffraction patterns, collective referred to by the generic name electron diffraction. This includes aspects...

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Diffraction

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coined the word diffraction and was the first to record accurate observations of the phenomenon in 1660. In classical physics, the diffraction phenomenon is...

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Le Bail method

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phase-purity. Generally, the intensities of powder diffraction data are complicated by overlapping diffraction peaks with similar d-spacings. For the Le...

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Silver behenate

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Centre for Diffraction Data round robin study of silver behenate. A possible low-angle X-ray diffraction calibration standard". Powder Diffraction. 10 (2):...

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Lanthanum hexaboride

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Material 660c Line Position and Line Shape Standard for Powder Diffraction (Lanthanum Hexaboride Powder)" https://tsapps.nist.gov/srmext/certificates/660c...

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Hugo Rietveld

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famous for his publication on the full profile refinement method in powder diffraction, which became later known as the Rietveld refinement method. The method...

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Scattering

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scattering Phase space measurement with forward modeling Photon diffusion Powder diffraction Raman scattering Rayleigh scattering Resonances in scattering from...

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Scherrer equation

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The Scherrer equation, in X-ray diffraction and crystallography, is a formula that relates the size of sub-micrometre crystallites in a solid to the broadening...

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Pozzolanic activity

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lower water to binder ratios (pastes), thermal analysis or X-ray powder diffraction techniques are commonly used to determine remaining calcium hydroxide...

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Crystallography

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crystals with different orientations). As such, powder diffraction techniques, which take diffraction patterns of samples with a large number of crystals...

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Ammonium nitrate

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Prask, H. J. (1983). "The structure of ND4NO3 phase V by neutron powder diffraction". Acta Crystallographica B. 39 (4): 414–420. Bibcode:1983AcCrB..39...

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Phases of ice

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and Raman The disordered nature of Ice IV was confirmed by neutron powder diffraction studies by Lobban (1998) and Klotz et al. (2003). In addition, the...

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Topas

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lascar ship's crew TOPAS, a software package used in the analysis of powder diffraction data Topass, a Portuguese ethnicity in the Indian Ocean Topa, a census...

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